Synthesis of N-nitrooxazolidines and N-nitrotetrahydro-1,3-oxazines from N-(2-hydroxyalkyl)- and N-(3-hydroxyalkyl)sulfamates期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

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Synthesis of N-nitrooxazolidines and N-nitrotetrahydro-1,3-oxazines from N-(2-hydroxyalkyl)- and N-(3-hydroxyalkyl)sulfamates

Authors:	V A Tartakovsky A S Ermakov Yu A Strelenko D B Vinogradov S A Serkov

Institution:	(1) N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991 Moscow, Russian Federation

Abstract:	A method was developed for the preparation of functionally substituted N-nitrooxazolidines and N-nitrotetrahydro-1,3-oxazines by nitration of the products obtained in the reactions of N-(2-hydroxyalkyl)- and N-(3-hydroxyalkyl)sulfamates with formaldehyde.

Keywords:	N-nitrooxazolidines N-nitrotetrahydro-1 3-oxazines N-(2-hydroxyalkyl)sulfamates N-(3-hydroxyalkyl)sulfamates formaldehyde nitration ¹H and ¹³C NMR spectroscopy 2D NMR spectroscopy IR spectroscopy mass spectrometry
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