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Temperature controlled synthesis of SrCO3 nanorods via a facile solid-state decomposition rout starting from a novel inorganic precursor |
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| Authors: | Fatemeh Davar Masoud Salavati-Niasari Sotirios Baskoutas |
| Institution: | a Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P. O. Box. 87317-51167, Islamic Republic of Iran b Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, P. O. Box. 87317-51167, Islamic Republic of Iran c Department of Materials Science, University of Patras, 26504 Patras, Greece |
| Abstract: | Strontium carbonate nanorods have been successfully synthesized via solid-state decomposition of a new precursor, Sr(Pht)(H2O)2]. The obtained nanorods were found to be orthorhombic with the length of 70-100 nm and the diameter of about 10-15 nm. The Effect of calcinations temperature on morphology and purity of the products has been investigated. Strontium carbonate nanorods were formed at 500 °C. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Fourier transform infrared (FT-IR) spectroscopy. In addition, further evidence for the purity and stoichiometry of the product was obtained by XPS (X-ray photoelectron spectroscopy) spectrum. |
| Keywords: | Inorganic precursor SrCO3 Phthalate Solid-state decomposition |
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