Thermal behaviour of [N(2-ammoniumethyl) piperazinium] pentachlorocuprate(II) dihydrate |
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Authors: | J Giusti G G T Guarini L Menabue G C Pellacani |
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Institution: | (1) Dipartimento di Chimica, Universitá di Firenze, Via G. Capponi 9, 50121, Firenze;(2) Istituto di Chimica Generale ed Inorganica, Universitá di Modena, Via G. Campi 183, 41100 Modena, Italy |
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Abstract: | The thermal behaviour of single-crystals of the title compound has been investigated by means of thermal methods supported by optical microscopy. A complex change takes place on heating. After the loss of the two water molecules, leading to an amorphous phase, recrystallization takes place. This results in a solid (probably an anhydrous form) which reacts further, through partial liquefaction, to yield a red crystalline product whose structure has been characterized via X-ray powder spectra and electronic and IR spectroscopy.
Zusammenfassung Das thermische Verhalten von Einkristallen der Titelverbindung wurden mittels thermischer Methoden und optischer Mikroskopie untersucht. Beim Erhitzen verläuft ein komplexer Prozeß. Nach dem zu einer amorphen Phase führenden Verlust von zwei Wassermolekülen findet eine Rekristallisation statt. Dabei wird eine feste Substanz, wahrscheinlich in wasserfreier Form, erhalten, die über partielle Verflüssigung unter Bildung eines roten kristallinen Produktes weiterreagiert, dessen Struktur durch Röntgenpulverspektren sowie Elektronen- und Infrarotspektroskopie charakterisiert wurde.
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