Synthesis of Pb8Pr2(GeO4)4(VO4)2 and refinement of its crystal structure |
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Authors: | N. V. Yablochkova |
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Affiliation: | 1274. Donetsk National University, ul. Universitetskaya 24, Donetsk, 83001, Ukraine
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Abstract: | The conditions of synthesis of lead praseodymium vanadatogermanate Pb8Pr2(GeO4)4(VO4)2 with an apatite structure were determined by X-ray powder diffraction. The elemental composition and homogeneity of the synthesized sample were verified by scanning electron microscopy. The crystal structure was refined by the Rietveld method. |
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