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Preparation of CdS nanowires by the decomposition of the complex in the presence of microwave irradiation
Authors:Jie He  Xiao-Ning Zhao  Jun-Jie Zhu and Jun Wang
Institution:

a Department of Chemistry, Laboratory of Mesoscopic Materials Science, Nanjing University, 210093 Nanjing, China

b Department of Chemical Engineering, Huainan Institute of Technology, Huainan 232001, China

Abstract:A novel synthetic route for the preparation of CdS nanowires has been developed. CdS nanowires with a diameter of ca. 4 nm have been successfully prepared by the microwave irradiation of a complex of cadmium-1-pyrrlidine dithio carboxylic acid ammonium (C5H12N2S2, APDTC) Cd(APDTC)2]2 in an ethylenediamine solution. The CdS nanowires were characterized by powder X-ray diffraction pattern, transmission electron microscopy (TEM), UV-Vis spectroscopy, diffuse reflection spectroscopy and PL spectroscopy.
Keywords:A1  Crystal morphology  A1  X-ray diffraction  A1  Nanostructures  B1  Sulfides  B1  Nanomaterials  B2  Semiconducting II–VI materials
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