| A Bidenate Amide Bonded Stationary Phase for HPLC |
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| 引用本文： | TianBaoHUANG YanShunMA YuanDeLONG YongLiangDING. A Bidenate Amide Bonded Stationary Phase for HPLC[J]. 中国化学快报, 2003, 14(8): 820-823 |
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| 作者姓名： | TianBaoHUANG YanShunMA YuanDeLONG YongLiangDING |
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| 作者单位： | ChengduInstituteofOrganicChemistry,ChineseAcademyofSciences,Chengdu610041 |
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| 摘 要： | A novel bonded stationary phase, bidenate amide bonded stationary phase (BABSP),was prepared by reacting YWG silica gel firstly with 3-aminopropyltrimethoxysilane, then with diacid chloride. Hydrophobicity, selectivity, and especially silanophilic activity of BABSP were evaluated. The stationary phase exhibited good column efficiency and peak shape for separation of some basic solutes.
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| 关 键 词： | 二齿氨基化合物 固相 HPLC 高性能流体色谱 硅烷醇 活性 疏水性 |
A Bidenate Amide Bonded Stationary Phase for HPLC |
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| Yan Shun MA,Yuan De LONG,Yong Liang DING,Tian Bao HUANG. A Bidenate Amide Bonded Stationary Phase for HPLC[J]. Chinese Chemical Letters, 2003, 14(8): 820-823 |
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| Authors: | Yan Shun MA Yuan De LONG Yong Liang DING Tian Bao HUANG |
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| Abstract: | A novel bonded stationary phase, bidenate amide bonded stationary phase (BABSP), was prepared by reacting YWG silica gel firstly with 3-aminopropyltrimethoxysilane, then with diacid chloride. Hydrophobicity, selectivity, and especially silanophilic activity of BABSP were evaluated. The stationary phase exhibited good column efficiency and peak shape for separation of some basic solutes. |
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| Keywords: | High performance liquid chromatography stationary phase silanophilic activity hydrophobicity. |
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