An investigation into causes and effects of high cyanide levels in the palladium-catalyzed cyanation reaction |
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| Authors: | Marcantonio Karen M Frey Lisa F Liu Yong Chen Yadan Strine Jeff Phenix Brian Wallace Debra J Chen Cheng-yi |
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| Affiliation: | Department of Process Research, Merck Research Laboratories, P.O. Box 2000 Rahway, New Jersey 07065, USA. karen_marcantonio@merck.com |
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| Abstract: | [reaction: see text] The palladium-catalyzed cyanation reaction is known to be sensitive to dissolved cyanide. Investigation into some causes of high levels of dissolved cyanide is presented here, along with a robust solution to this problem. |
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