Comments on ‘Unusual oxidative rearrangement of 1,5-diazadecalin’ |
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| Authors: | Tammo Winkler |
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| Institution: | Syngenta Crop Protection AG, CH 4002 Basel, Switzerland |
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| Abstract: | Oxidation of cis or trans 1,5-diazadecalin with (PhIO)n yields 2-pyrrolidinone and not 1,6-diaza-2,7-cyclodecadione, as reported. This is shown by a comparison of the NMR data of the reaction product with those of 2-pyrrolidinone and 1,6-diaza-2,7-cyclodecadione. |
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| Keywords: | Diazadecalins Macrocyclic bislactams NMR Conformational analysis |
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