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热蒸发法制备的球棒状氧化锌晶体的形貌及生长过程
引用本文:高品,王凯,黄超,孟路,徐法强.热蒸发法制备的球棒状氧化锌晶体的形貌及生长过程[J].化学物理学报,2016,29(3):369-373.
作者姓名:高品  王凯  黄超  孟路  徐法强
作者单位:中国科学技术大学合肥国家同步辐射实验室, 合肥 230026,中国科学技术大学合肥国家同步辐射实验室, 合肥 230026,中国科学技术大学合肥国家同步辐射实验室, 合肥 230026,中国科学技术大学合肥国家同步辐射实验室, 合肥 230026,中国科学技术大学合肥国家同步辐射实验室, 合肥 230026
基金项目:This work is supported by Scienti c Research Grant of Hefei Science Center of Chinese Academy of Science (No.2015SRG-HSC032) and the National Natural Sci-ence Foundation of China (No.U1232137).
摘    要:在不用催化剂的条件下,通过热蒸发锌粉的方法,一种新颖的球棒状的氧化锌纳米结构被沉积在硅基片上.每一根球棒状的氧化锌纳米棒("纳米球棒")由三部分构成,分别是六边形"球棒头"、"球棒把手"以及一个连接过渡的部分.高分辨率透射电镜和选区电子衍射结果表明,纳米棒呈单晶特性,沿着0001]方向择优生长.根据对实验结果的分析,纳米球棒的生长过程可以利用气-固生长机制进行解释,合理地提出其生长模型.

关 键 词:氧化锌  热蒸发  纳米结构  生长过程
收稿时间:2015/12/22 0:00:00
修稿时间:2016/2/25 0:00:00

Morphology and Growth Process of Bat-like ZnO Crystals by Thermal Evaporation
Pin Gao,Kai Wang,Chao Huang,Lu Meng and Fa-qiang Xu.Morphology and Growth Process of Bat-like ZnO Crystals by Thermal Evaporation[J].Chinese Journal of Chemical Physics,2016,29(3):369-373.
Authors:Pin Gao  Kai Wang  Chao Huang  Lu Meng and Fa-qiang Xu
Institution:National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230026, China,National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230026, China,National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230026, China,National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230026, China and National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230026, China
Abstract:A novel bat-like ZnO nanostructure was synthesized on the silicon substrate by simple ther-mal evaporation of zinc powders without any catalyst. Each bat-like nanorod ("nanobat") is composed of a hexagonal head, a continuous neck and a thin handle. High-resolution transmission electron microscopy and selected area electron di raction results reveal the single-crystalline feature and the growing direction along 0001] of the nanobat. The vapor-solid mechanism was found suitable to explain the growth process of the nanobat and a schematic model was proposed in detail based on the experimental results.
Keywords:ZnO  Thermal evaporation  Nanostructure  Growth process
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