| 氢化物发生-双道原子荧光光谱法同时测定钢中砷和锑 |
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| 引用本文： | 曾勤.氢化物发生-双道原子荧光光谱法同时测定钢中砷和锑[J].分析测试技术与仪器,2008,14(1):23-25. |
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| 作者姓名： | 曾勤 |
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| 作者单位： | 福建龙溪轴承(集团)股份有限公司检测实验中心,福建,漳州,363000 |
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| 摘 要： | 建立了一种氢化物发生双道原子荧光光谱法同时测定钢中痕量砷和锑的方法．对实验条件进行了优化，在最佳工作条件下，砷和锑的检出限分别为0．012ng／g和0．034ng／g，RSD分别为1．24％和1．97％．将本法应用于钢中的砷和锑的测定，采用加标回收实验控制方法的准确性，砷的回收率为96％～98％，锑的回收率98％～102％．
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| 关 键 词： | 双道原子荧光光谱法 砷 锑 钢 |
| 文章编号： | 1006-3757(2008)01-0023-03 |
| 收稿时间： | 2008/1/14 0:00:00 |
| 修稿时间： | 2008年1月14日 |
Simultaneous Determination of Arsenic and Antimony in Steel by Double Channel Atomic Fluorescence Spectrometry with Hydride Generation Technique |
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| ZENG Qin.Simultaneous Determination of Arsenic and Antimony in Steel by Double Channel Atomic Fluorescence Spectrometry with Hydride Generation Technique[J].Analysis and Testing Technology and Instruments,2008,14(1):23-25. |
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| Authors: | ZENG Qin |
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| Institution: | ZENG Qin (Measuring and Testing Center of Fujian Longxi Bearing (Group) Corporation Limited, Zhangzhou 363000, China) |
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| Abstract: | A analytical method was proposed for simultaneous determination of arsenic and antimony in steel by hydride generation double channel atomic fluorescence spectrometry.Under optimized conditions,the determination limits of arsenic and antimony were 0.012 ng/g and 0.034 ng/g,respectively.RSD were 1.24% and 1.97%.The experiment of spiked recovery was carried out in order to validate the method.The recovery was from 96% to 98% for arsenic,98% to 102% for antimony. |
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| Keywords: | double channel-atomic fluorescence spectrometry arsenic antimony steel |
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