| 微波场下水滑石的快速合成及制备 |
| |
| 引用本文： | 贺鹤鸣 蒋大振. 微波场下水滑石的快速合成及制备[J]. 高等学校化学学报, 1992, 13(11): 1462-1463 |
| |
| 作者姓名： | 贺鹤鸣 蒋大振 |
| |
| 作者单位： | 吉林大学化学系 长春130023(贺鹤鸣，蒋大振)，吉林大学化学系 长春130023(孙铁) |
| |
| 摘 要： | 水滑石以其独特的碱催化性能~[1,2]、记忆效应及阴离子交换~[3]等特性引起人们的关注,其合成多用水热法.本文研究了在微波场中水滑石的合成及制备,得到了较好的结果. 1 实验部分 1.1 仪器与试剂 Shimadzu CD-3A型X射线衍射仪(日本);Nicolet 5DX FTIR光谱仪(美国),KBr压片;蚬华E100-EA型微波炉(广东顺德).所有试剂均为分析纯.
|
| 关 键 词： | 水滑石 类水滑石 微波 交联 |
Preparation and Synthesis of Hydrotalc in Microwave Field |
| |
| HE He-Ming,JIANG Da-Zhen,SUN Tie. Preparation and Synthesis of Hydrotalc in Microwave Field[J]. Chemical Research In Chinese Universities, 1992, 13(11): 1462-1463 |
| |
| Authors: | HE He-Ming JIANG Da-Zhen SUN Tie |
| |
| Abstract: | The present study reports the synthesis of hydrotalc and hydrotalc-like substance by microwave method,which was compared with that of the conventional hydrothermal method.The microwave method gave a good quality product rapidly.By the characterization of XRD and IR,it was found that the hydrotalc can be intercalated easily and exchanged completely with anions.The intercalating products possess a long-range order. |
| |
| Keywords: | Hydrotalc Hydrotalc-like Microwave Intercalation |
| 本文献已被 CNKI 维普 等数据库收录！ |
