| 新型尾式硫代苯并噻唑基卟啉化合物的合成与表征 |
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| 引用本文： | 刘新刚,冯亚青,高博,周立山. 新型尾式硫代苯并噻唑基卟啉化合物的合成与表征[J]. 有机化学, 2005, 25(5): 540-544 |
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| 作者姓名： | 刘新刚 冯亚青 高博 周立山 |
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| 作者单位： | 天津大学化工学院,天津,300072 |
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| 摘 要： | 通过不对称的单羟基卟啉化合物、溴代烷烃和巯基苯并噻唑合成了一系列新型硫代苯并噻唑基尾式卟啉化合物, 并采用核磁共振氢谱、碳谱、红外光谱、质谱和元素分析对卟啉化合物的结构进行了表征.
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| 关 键 词： | 尾式卟啉 巯基苯并噻唑 合成 表征 |
| 收稿时间： | 2004-03-22 |
| 修稿时间： | 2004-11-14 |
Synthesis and Characterization of Novel 2-Thiobenzo[d]thiazole Tailed-porphyrin |
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| LIU Xin-Gang,FENG Ya-Qing,GAO Bo,ZHOU Li-Shan. Synthesis and Characterization of Novel 2-Thiobenzo[d]thiazole Tailed-porphyrin[J]. Chinese Journal of Organic Chemistry, 2005, 25(5): 540-544 |
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| Authors: | LIU Xin-Gang FENG Ya-Qing GAO Bo ZHOU Li-Shan |
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| Affiliation: | (School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072) |
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| Abstract: | A series of new 2-thiobenzo[d]thiazole-linked tailed porphyrins were synthesized by the un- symmetrical monohydroxyporphyrins with alkyl bromides followed by treatment with 2-thiobenzo- [d]thiazole. And their structures were confirmed by IR, 1H NMR, 13C NMR, MS spectra and elemental analysis. |
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| Keywords: | tailed porphyrin 2-thiobenzo[d]thiazole synthesis structure identification |
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