|
|||||
|
|
Simplification of determination method for standard materials using post-column reaction GC/FID |
|
| Authors: | Takuro Watanabe Kenji Kato Nobuhiro Matsumoto Tsuneaki Maeda |
| Affiliation: | aOrganic Standards Section 1, Organic Analytical Chemistry Division, National Metrology Institute of Japan (NMIJ), National Institute of Advanced Industrial Science and Technology (AIST), AIST Tsukuba Central 3-10, 1-1-1 Umezono, Tsukuba, Ibaraki 305-8563, Japan bNational Metrology Institute of Japan (NMIJ), National Institute of Advanced Industrial Science and Technology (AIST), AIST Tsukuba Central 5-2, 1-1-1 Higashi, Tsukuba, Ibaraki 305-8565, Japan |
| Abstract: | For the simple and fast preparation of highly reliable standard materials, a post-column reaction GC/FID system was developed and evaluated on the mixture of oxygen-containing organic compounds. The oxygen-containing organic compounds mixing solution were determined with the post-column reaction GC/FID system using n-dodecane as an internal calibration standard. Required value of relative expanded uncertainty as an original source of SI-traceable standard materials was within 1% and it aimed at this value as accuracy of the quantitative analysis. The results showed good agreement between the prepared concentrations and analytical values using post-column reaction GC/FID system. These results indicated that the post-column reaction GC/FID system would be used for getting SI-traceable values. |
| Keywords: | GC/FID Post-column reaction Standard material Oxygen-containing organic compound |
| 本文献已被 ScienceDirect 等数据库收录！ | |