Determination of enantiomeric purity of 1-substituted 3-amino-1,2-dicarba-closo-dodecaboranes by HPLC on chiral stationary phases |
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| Authors: | V. P. Krasnov A. M. Demin G. L. Levit A. N. Grishakov L. Sh. Sadretdinova V. A. Ol’shevskaya I. V. Glukhov V. N. Kalinin V. N. Charushin |
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| Affiliation: | (1) Analytical Research, Custom Pharmaceutical Services, Dr. Reddy’s Laboratories, Hyderabad, 500049, India;(2) Process Research, Custom Pharmaceutical Services, Dr. Reddy’s Laboratories, Hyderabad, 500049, India;(3) Department of Chemistry, J.N.T.U. College of Engineering, Anantapur, 515002, India; |
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| Abstract: | A determination of enantiomeric purity of 1-substituted (Me, Ph, and Pri) 3-amino-1,2dicarba-closo-dodecaboranes by HPLC on chiral Chiralcel OD-H and Chiralpac AD stationary phases involving preliminary phthaloylation of 3-aminocarboranes has been suggested as a general method. |
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