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Laboratory set-up for X-ray diffraction at high pressures
Authors:Catalin Popescu  Loreynne Pinsard-Gaudart  Nita Dragoe
Affiliation:1. Univ Paris-Sud , UMR 8182, 91405, Orsay, France;2. CNRS , 91405, Orsay, France catalin.popescu@u-psud.fr;4. CNRS , 91405, Orsay, France
Abstract:We describe here a simple set-up for X-ray diffraction under high pressure using a diamond anvil cell employing a sealed tube. The set-up works in angular dispersive geometry and is built using rather common components that are available in a research laboratory. We show that using this set-up one can routinely acquire good-quality data for the determination of structural properties under pressure and the equations of state. Technical details are presented along with examples of experimental results for sodium chloride and LiV2O4.
Keywords:X-ray diffraction  laboratory set-up  diamond anvil cell  high pressure
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