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Diamond anvils with a spherical support designed for X-ray and neutron diffraction experiments in DAC
Authors:N. Dubrovinskaia  L. Dubrovinsky  M. Hanfland  M. Hofmann
Affiliation:1. Material Physics and Technology at Extreme Conditions, Laboratory of Crystallography , Universit?t Bayreuth , 95440 , Bayreuth , Germany natalia.dubrovinskaia@uni-bayreuth.de;3. Bayerisches Geoinstitut , Universit?t Bayreuth , 95440 , Bayreuth , Germany;4. ESRF , Bo?te Postale 220, 38043 , Grenoble , France;5. Forschungs-Neutronenquelle Heinz Maier-Leibnitz (FM II) , TU München, 85747 , Garching , Germany
Abstract:Here, we present new diamond anvils with a spherical support designed for applications in diamond anvil cell (DAC) technique. The main feature of the anvils is the diamond crown of a spherical shape. The assembly of the spherical diamond fixed within a spherical support of a seat made of tungsten carbide or hard metals provides enhanced stability, simple alignment, and large optical and X-ray aperture that makes it very useful for broad applications in DAC technique, particularly for single crystal X-ray and powder neutron diffraction. The anvils were tested in various experiments conducted in a wide pressure–temperature range and showed a very good performance.
Keywords:diamond anvil cell technique  high pressure generation  spherical diamonds  X-ray diffraction  neutron diffraction
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