Preparation and chiral separation of a novel immobilized cellulose-based chiral stationary phase in high-performance liquid chromatography |
| |
| Authors: | Peng Gui Ming Wu Su Qin Fang Zhi Li Zhang Wei Guang Zhang Zhen Bin Fan Jun Zheng Sheng Run Wu Shang Sen Ng Siu Choon |
| |
| Institution: | School of Chemistry and Environment, South China Normal University, Guangzhou, 510006, China. |
| |
| Abstract: | The chiral selector 6-azido-2, 3-di(p-chlorophenylcarbamoylated) cellulose was synthesized and further chemically immobilized onto 5-μm amino functionalized spherical porous silica gel. It was used as chiral stationary phase in high-performance liquid chromatography. Thirty racemates were successfully separated into enantiomers in either normal phase mode or reversed-phase mode. Good reproducibility and stability of the chiral stationary phase have been demonstrated. |
| |
| Keywords: | |
| 本文献已被 PubMed 等数据库收录！ |
|
