Development of a method for des-glaucine production in a subcritical water medium |
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| Authors: | S N Borisenko A V Bicherov O V Pavlyuk M I Rudnev N I Borisenko E V Vetrova V I Minkin R N Borisenko A V Lekar |
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| Institution: | (1) Department of Materials and Interfaces, Weizmann Institute of Science, 76100 Rehovot, Israel |
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| Abstract: | The isomerization of a non-racemic mixture of glaucine isomers to des-glaucine (seco-glaucine) in a subcritical water medium
at 200–300°C was conducted with a yield of 53%. The structure of the product was confirmed by NMR spectroscopy and electrospray-ionization
mass spectrometry. |
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