Abstract: | A novel reaction to synthesis a series new N‐hydroxyldecahydroacridine derivatives by a one‐pot condensation of aldehyde, 1,3‐dicarbonyl compound and NH2OH in glycol under microwave irradiation is described. N‐hydroxyldecahydroacridine was obtained in excellent yields (81–95%) within short reaction time (4–7 min) |