2-Nitromethyl-2-trichloromethyl-1,3-benzodioxoles and 2-nitromethyl-2-trichloromethyl-1,3-benzoxazolines: Synthesis and structure |
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| Authors: | S V Makarenko E V Stukan’ K A Lyssenko I V Anan’ev V M Berestovitskaya |
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| Institution: | 1. Herzen State Pedagogical University of Russia, 48 nab. r. Moiki, 191186, Saint Petersburg, Russian Federation
2. A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 ul. Vavilova, 119991, Moscow, Russian Federation
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| Abstract: | A reaction of 1-bromo-3,3,3-trichloro-1-nitropropene with pyrocatechol, o-aminophenol, and their substituted derivatives led to 2-nitromethyl-2-trichloromethyl-1,3-benzodioxoles and 2-nitromethyl-2-trichloromethyl-1,3-benzoxazolines. The structure of the compounds synthesized was established by IR, 1H and 13C NMR spectroscopy with HMQC and HMBC 1H—13C experiments, and X-ray diffraction analysis. |
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