| 茚酮肟醚的合成 |
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| 引用本文： | 彭杨,朱必敏,程鹏,曾庆东,余瑜.茚酮肟醚的合成[J].光谱实验室,2013,30(5):2399-2402. |
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| 作者姓名： | 彭杨 朱必敏 程鹏 曾庆东 余瑜 |
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| 作者单位： | 重庆医科大学药学院 重庆市渝中区医学院路1号 400016 |
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| 摘 要： | 以1-茚酮为原料,经盐酸羟胺缩合得到1-茚酮肟,通过溴丙炔取代等得到产物.重点考察了溴丙炔取代的反应温度、反应时间、催化剂.该方法操作简单、成本低、目标产物收率较高,适合于工业化生产.
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| 关 键 词： | 茚酮肟醚 取代 结构表征 优化 |
Synthesis And Characterization of (Z)-2,3-dihydroind-en-1-one ON-prop-2-ynyloxyme |
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| PENG Yang
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ZHU Bi-Min
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CHENG Peng
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ZENG Qing-Dong
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YU Yu.Synthesis And Characterization of (Z)-2,3-dihydroind-en-1-one ON-prop-2-ynyloxyme[J].Chinese Journal of Spectroscopy Laboratory,2013,30(5):2399-2402. |
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| Authors: | PENG Yang ZHU Bi-Min CHENG Peng ZENG Qing-Dong YU Yu |
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| Institution: | (College of Pharmaceutical Sciences, Chongqing Medical University, Chongqing, 400016, P. R. China) |
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| Abstract: | （Z）-2, 3-dihydroind-en-l-one ON-prop- 2-ynyloxyme was synthesized from 1-indanone and hydroxylamine hydrochloride by condensation, alklation with bromopropyne, The substituted reaction temperature,reaction time and catalyst was investigated. The method is simple, lower cost and a higher yield of the target product,suitable for industrial production. |
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| Keywords: | Indanone Oxime Ether Substitution Structural Characterization Optimization |
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