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Bestimmung der Empfindlichkeit bei Tc-99-NMR-Messungen an einem 250-MHz-Spektrometer
Authors:M Findeisen  B Lorenz  M Wahren
Abstract:By means of different concentrations the signal-to-noise ratios of Tc-99-NMR spectra were determined applying well measurable Tc-samples tetrabutylammoniwn pertechnetate, TBA (TcO4)J and a 250 MHz-spectrometer. The signal-to-noise ratios of the spectra were determined by using the integrated routines of the firm's software and accumulating different number of scans. By fittings of data of the signal-to-noise ratio dependence and by extrapolation the minimum Tc-concentralion could be empirically found out. Applying a duration of measurements of 12 hours about 10?7 molar concentrations can be determined.
Keywords:accuracy  computers  nuclear magnetic resonance  quantity ratio  technetium compounds  technetium 99  sensitivity  signal-to-noise ratio
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