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Use of graphite to improve heat determinations by differential scanning calorimetry
Authors:G. G. T. Guarini  R. Spinicci  D. Donati
Affiliation:(1) Institute of Physical Chemistry, University of Florence, Firenze;(2) Centro di studio del C.N.R sulla chimica e la struttura dei composti eterociclici e loro applicazioni, University of Florence, c/o Institute of Organic Chemistry, Firenze, Italy
Abstract:The presence of graphite is demonstrated to reduce the influence of thermal emissivity on the evaluation of heat changes for reactions of the type: Asolid rarr Bsolid + Cgas by differential scanning calorimetry.Work supported, by the Italian Consiglio Nazionale delle Ricerche (C.N.R.).
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