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Natural abundance 13C - 13C coupling constants observed via double quantum coherence. Structural elucidation by the one- and the two-dimensional NMR experiements of velloziolone,a new seco-diterpene.
Authors:Angelo C. Pinto  Susan K. Do Prado  Raimundo Braz Filho  William E. Hull  Andras Neszmelyi  Gabor Lukacs
Affiliation:1. Universidade Federal do Rio de Janeiro, Nucleo de Pesquisas de Produtos Naturais, 21941 Rio de Janeiro Brazil;2. Bruker Analytische Messtechnik, Am Silberstreifen, D-7512 Rheinstetten-Fo Germany;3. Central Research Institute for Chemistry of the Hungarian Academy of Sciences, H-1025 Budapest, Pusztaszeri ut Hungary;4. Institut de Chimie des Substances Naturelles du CNRS, 91190 Gif-sur-Yvette France
Abstract:With the help of Natural Abundance 13C - 13C Coupling Constants, observed via double quantum coherence, the structural determination of VELLOZIOLONE (1), a new diterpene, has been carried out.
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