Development of a miniature simultaneous MPT spectrometer |
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Authors: | Guodong Feng Yanfu Huan Yanbo Cao Shuhua Wang Xinghua Wang Jie Jiang Aimin Yu Qinhan Jin Hongmei Yu |
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Affiliation: | a Institute of Analytical Science, School of Chemistry, Jilin University, Jilin Province Research Center for Engineering and Technology of Spectral Analytical Instruments, Changchun 130023, PR China;b Net Center, Jilin University, Changchun 130012, PR China |
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Abstract: | An unique miniature simultaneous microwave plasma torch (MPT) atomic emission spectrometer employing linear UV intensified charge-coupled device (ICCD) array detector has been developed and studied preliminarily. The detection limits and precisions of the spectrometer for Ag, Al, Ba, Ca, Cr, Cu, Fe, Mg, Mn, Sr and V by using different CCD exposure times have been determined. An analysis of a practical sample has been carried out. The preliminary results demonstrate that such simultaneous spectrometer has advantages of saving sample and time, especially suitable for use as detector for chromatography and in combination with flow injection systems. Taking analytical figures of merit and portability into accounts, the miniature simultaneous MPT system will have extended application areas and greater competition potential as compared with commercialized scanning MPT spectrometers. |
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Keywords: | Author Keywords: Microwave plasma torch Simultaneous spectrometer Linear UV intensified charge-coupled device (ICCD) detector |
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