Influence of process parameters on the epoxidation of 2-buten-1-ol over titanium silicalite TS-1 catalyst |
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Authors: | Agnieszka Wróblewska Ewelina Ławro Eugeniusz Milchert |
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Affiliation: | (1) Institute of Organic Chemical Technology, Szczecin University of Technology, ul. Pulaskiego 10, PL-70-322 Szczecin, Poland |
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Abstract: | The influence of process parameters on the epoxidation of 2-buten-1-ol with 30 % hydrogen peroxide using the titanium silicalite TS-1 is presented. The studies were carried out under autogenic pressure (in autoclave). Methanol was used as a solvent in this process. The influence of temperature, 2-buten-1-ol to hydrogen peroxide mole ratio, amount of solvent used, TS-1 catalyst content, and reaction time on the reaction was studied. The major product of this reaction, 2,3-epoxybutan-1-ol (EB), has numerous applications in chemical industry. |
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Keywords: | 2,3-epoxybutan-1-ol epoxidation titanium silicalite |
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