Analysis by calorimetry |
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Authors: | Bernhard Wunderlich |
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Institution: | Department of Chemistry, Rensselaer Polytechnic Institute, Troy, N.Y. 12181 U.S.A. |
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Abstract: | The last years have seen the development of differential calorimetry into a scanning technique for routine analysis. In order of ease of determination heats of fusion, heats of reaction, phase diagrams, purity analysis, heat capacity and similar heat effects are added to the list of quickly measurable quantities. Accuracies of the order of 1–5% of heats of fusion and heat capacity are obtainable under favorable conditions. Special topics which have been discussed are instrumentation, transition temperatures, heat capacities, glass transitions, heats of transitions, and phase diagrams. |
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