| 固体酸AlCl3/D001催化合成苹果酯的研究 |
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| 引用本文： | 陶贤平.固体酸AlCl3/D001催化合成苹果酯的研究[J].合成化学,2003,11(1):86-88. |
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| 作者姓名： | 陶贤平 |
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| 作者单位： | 南通职业大学化学工程系,江苏,南通,226007 |
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| 摘 要： | 以AlCl3/D001催化乙酰乙酸乙酯和乙二醇反应合成苹果酯，反应条件：乙酰乙酸乙酯1．0mol，乙二醇1．6mol,苯150mL,AlCl3.D001 7g，反应时间3h，苹果脂收率82．3％。
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| 关 键 词： | AlCl3／D001 苹果酯 固体酸 催化合成 香精 催化剂 氯化铝 D001树脂 |
| 文章编号： | 1005-1511(2003)01-086-03 |
| 修稿时间： | 2002年6月29日 |
Studies on Synthesis of Fructone Using Solid Acid Catalyst AlCl3/D001 |
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| TAO,Xian-ping.Studies on Synthesis of Fructone Using Solid Acid Catalyst AlCl3/D001[J].Chinese Journal of Synthetic Chemistry,2003,11(1):86-88. |
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| Authors: | TAO Xian-ping |
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| Abstract: | Fructone was synthesized by reaction of ethyl acetyl acetate and ethyleneglycol using AlCl 3/D001 as a catalyst. The optimum conditions were found out as follows: the ratio of ethyl acetyl acetate to ethyleneglycol to benzene to AlCl 3/D001 was 1.0mol to 1.6mol to 7g for 3h. On these conditions the yield reached 82.3%. |
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| Keywords: | fructone solid acid catalysis synthesis |
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