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Solvothermal Synthesis of Molybdenum Disulfide Hollow Spheres Modified by Cyanex 301 in Water–Ethanol Medium
Authors:Xun Fu  Danmei Wu  Xiaodong Zhou  Huaqiang Shi  Zhengshui Hu
Institution:(1) Qingdao University of Science and Technology, Qingdao, Shandong, 266042, P. R. China
Abstract:Hollow spherical molybdenum disulfide has been successfully synthesized via a solvothermal method using Cyanex 301 as sulfur source and modification agent. The hollow spheres are characterized by transmission electron microscopy, scanning electron microscopy, X-ray diffraction and Energy-Dispersive X-ray analysis. The influences of reaction conditions are also discussed while a mechanism is proposed to explain the formation of the peculiar morphology.
Keywords:molybdenum disulfide  hollow spheres  solvothermal synthesis  nanoparticles  colloids
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