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One Pot Preparation of Amides from Azo Compounds by Sm/TiCl4
Authors:Xue Li  Yong‐Min Zhang
Abstract:Azo compounds were conveniently reduced by a system consisting of Sm/TiCl4 to produce aniline anions. This anion species reacted smoothly with aliphatic acyl chlorides or acid anhydrides to afford corresponding amides under mild and neutral conditions.
Keywords:Amides  Azo compound  Sm/TiCl4  Reduction
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