Synthesis and Tautomeric Equilibrium of Polyfluoroacyl-Containing 1,5-Benzodiazepines |
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| Authors: | Danil S Yachevskii Dmitry L Chizhov Mikhail I Kodess and Kazimir I Pashkevich |
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| Institution: | (1) Favorsky Irkutsk Institute of Chemistry, Irkutsk, Russian;; |
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| Abstract: | The reaction of bis(polyfluoroalkyl)-containing 1,3,5-triketones with o-phenylenediamine yielded 2-polyfluoroacylmethylene-4-polyfluoroalkyl-1,3- or 1,5-dihydro-1,5-benzodiazepines. The tautomeric equilibrium of the obtained benzodiazepines in CDCl3, CD3CN, DMSO, and DMF solution was studied. |
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