Solid state reactions of nitrogenous heterocyclic compounds(Ⅰ)——Solid state reactions of 3-methyl-l-phenyl-5-pyrazolone with carbonyl compounds |
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引用本文: | 李晓陆,杜大明,王永梅,孟继本.Solid state reactions of nitrogenous heterocyclic compounds(Ⅰ)——Solid state reactions of 3-methyl-l-phenyl-5-pyrazolone with carbonyl compounds[J].中国科学B辑(英文版),1997(2). |
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作者姓名: | 李晓陆 杜大明 王永梅 孟继本 |
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作者单位: | Department of Chemistry,Nankai University,Tianjin 300071,China,Department of Chemistry,Nankai University,Tianjin 300071,China,Department of Chemistry,Nankai University,Tianjin 300071,China,Department of Chemistry,Nankai University,Tianjin 300071,China |
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基金项目: | Project supported by the National Natural Science Foundation of China |
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摘 要: | The solid state reaction of 3-methyl-1-phenyl-5-pyrazolone (MPP) with aromatic aldehydes and ke-tones benzil derivatives and imides,and the solid state Michael addition reaction of MPP with 4-arylidene-3-methyl-1-phenyl-5-pyrnzolone 2 were investigated.Some new solid state reactions between the reactants were found,from which a series of new compounds were obtained The structures of the products were identified by IR,1H NMR,MS,elemental analyses and also by X-ray crystal analysis,and the reaction mechanism of MPP with aromatic aldehydes and ketones was proposed
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