| 微波辐射下Zr(SO4)2·4H2O/SiO2催化合成芳香磺酰亚胺 |
| |
| 引用本文： | 耿丽君,刘妍. 微波辐射下Zr(SO4)2·4H2O/SiO2催化合成芳香磺酰亚胺[J]. 有机化学, 2005, 25(9) |
| |
| 作者姓名： | 耿丽君 刘妍 |
| |
| 作者单位： | 邯郸学院化学系,邯郸,056005 |
| |
| 摘 要： | 微波辐射无溶剂条件下,以Zr(sO4)2·4H2O/SiO2固体酸为催化剂,芳香醛与芳香磺酰胺反应合成了一系列芳香磺酰亚胺化合物.此方法具有操作简便,催化剂价廉易得、活性高、可回收重复使用、对环境友好等优点.
|
| 关 键 词： | 芳香磺酰亚胺 芳香醛 芳香磺酰胺 微波辐射 |
A Solvent-free Procedure for Synthesis of N-Sulfonylimines Catalyzed by Zr(SO4)2·4H2O/SiO2 Solid Acid under Microwave Irradiation |
| |
| GENG,Li-Jun,LIU,Yan. A Solvent-free Procedure for Synthesis of N-Sulfonylimines Catalyzed by Zr(SO4)2·4H2O/SiO2 Solid Acid under Microwave Irradiation[J]. Chinese Journal of Organic Chemistry, 2005, 25(9) |
| |
| Authors: | GENG Li-Jun LIU Yan |
| |
| Abstract: | A manipulative simple and rapid procedure for the synthesis of N-sulfonylimines from aldehydes with sulfonamides was described. The reaction was conducted under microwave irradiation conditions in the absence of solvent using Zr(SO4)2?4H2O/SiO2 solid acid as catalyst . This solid acid is cheap, highly-active, chemically green and reusable. |
| |
| Keywords: | N-sulfonylimine aromatic aldehyde sulfonamide microwave irradiation |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
