| Synthesis and Crystal Structure of a Genistein-derived Compound |
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| 作者姓名： | ZHANG Li-N SHI Lei FANG Rui-Qin ZHU Hai-Liang |
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| 作者单位： | School of Life Sciences，Nanjing University，Nanjing 210093，China |
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| 摘 要： | A genistein derivative, 5-hydroxy-3-（4-hydroxyphenyl）-7-（2-（piperidin- 1-yl）ethoxy）- 4H-chromen-4-one 3, was designed, prepared and structurally characterized by single-crystal X-ray diffraction. X-ray structure analysis reveals that 3 crystallizes in the orthorhombic system, space group Pbca, with a = 16.238（3）, b = 10.308（2）, c = 22.987（5）A, V = 3847.6（13）A3, Z = 8,μ= 0.093 mm^-1, Dc = 1.317 g/cm^3, F（000） = 1616, R = 0.0789 and wR = 0.1554 for 1463 observed reflections with I 〉 2σ（I）.
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| 关 键 词： | 合成 晶体结构 染料木碱 1 2-二溴乙烷 哌啶 |
| 收稿时间： | 2007-03-27 |
| 修稿时间： | 2007-05-28 |
Synthesis and Crystal Structure of a Genistein-derived Compound |
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| ZHANG Li-N SHI Lei FANG Rui-Qin ZHU Hai-Liang.Synthesis and Crystal Structure of a Genistein-derived Compound[J].Chinese Journal of Structural Chemistry,2008,27(2):200-204. |
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| Authors: | ZHANG Li-Na SHI Lei FANG Rui-Qin ZHU Hai-Liang |
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| Institution: | School of Life Sciences, Nanjing University, Nanjing 210093, China |
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| Abstract: | A genistein derivative,5-hydroxy-3-(4-hydroxyphenyl)-7-(2-(piperidin-1-yl)ethoxy)-4H-chromen-4-one 3,was designed,prepared and structurally characterized by single-crystal X-ray diffraction.X-ray structure analysis reveals that 3 crystallizes in the orthorhombic system,space group Pbca,with a=16.238(3),b=10.308(2),c=22.987(5)(A),V=3847.6(13)(A),Z=8,μ=0.093 mm-1,Dc=1.317 g/cm3,F(000)=1616,R=0.0789 and wR=0.1554 for 1463observed reflections with,I＞2σ(I). |
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| Keywords: | genistein crystal structure derivative 1 2-dibromoethane piperidine |
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