| 稀土与水杨醛-1H-苯并三唑乙酰腙配合物的合成及抑菌实验 |
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| 引用本文： | 何水样,胡亭,杨锐,赵建社,薛岗林,史启祯. 稀土与水杨醛-1H-苯并三唑乙酰腙配合物的合成及抑菌实验[J]. 应用化学, 2003, 20(3): 205-0 |
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| 作者姓名： | 何水样 胡亭 杨锐 赵建社 薛岗林 史启祯 |
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| 作者单位： | 西北大学 |
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| 基金项目： | 陕西省自然科学基金 ( 0 2H0 10 )，北京大学稀土材料化学及应用国家重点实验室资助课题 |
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| 摘 要： | SBTH;生物活性;稀土与水杨醛-1H-苯并三唑乙酰腙配合物的合成及抑菌实验
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| 关 键 词： | SBTH 生物活性 稀土与水杨醛-1H-苯并三唑乙酰腙配合物的合成及抑菌实验 |
| 文章编号： | 1000-0518(2003)03-0205-05 |
| 收稿时间： | 2009-06-29 |
| 修稿时间： | 2002-06-19 |
Synthesis and Antibacterial Activity of Salicylaldehyde-1H-benzotriazol-1-acetyl hydrazone Complexes with Lanthanide Perchlorate |
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| HE Shui Yang ,HU Ting,YANG Rui,ZHAO Jian She,XUE Gang Lin,SHI Qi Zhen. Synthesis and Antibacterial Activity of Salicylaldehyde-1H-benzotriazol-1-acetyl hydrazone Complexes with Lanthanide Perchlorate[J]. Chinese Journal of Applied Chemistry, 2003, 20(3): 205-0 |
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| Authors: | HE Shui Yang HU Ting YANG Rui ZHAO Jian She XUE Gang Lin SHI Qi Zhen |
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| Affiliation: | HE Shui Yang *,HU Ting,YANG Rui,ZHAO Jian She,XUE Gang Lin,SHI Qi Zhen |
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| Abstract: | Salicylaldehyde 1H benzotriazol 1 acetyl hydrazone(C 15 H 13 N 5 O 2 , H 2L,SBTH) and its seven complexes with lanthanide perchlorates RE(HL) 2 ClO 4 (RE=Pr,Nd,Sm,Eu,Gd,Tb and Dy) have been synthesized and confirmed by elemental analysis, chemical analysis and molar conductivity measurement. The IR, UV and 1 H NMR results indicate that the SBTH is bonded with RE 3+ via the carbonyl and phenol oxygen and imidogen nitrogen, forming a pentacyclic and hexacyclic tridentate complex. The complexes show a certain antibacterial activity against leaf mold , bacilli and actinomyceto . |
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| Keywords: | rare earth salicylaldehyde benzotriazol acetyl hydrazone complex synthesis bioactivity |
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