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Determination of boron concentration in borosilicate glass,boron carbide and graphite samples by conventional wet-chemical and nuclear analytical methods
Authors:K Venkatesh  Sumit Chhillar  Granthali S Kamble  Shailaja P Pandey  Manisha Venkatesh  Sanjukta A Kumar  Sanjiv Kumar  R Acharya  P K Pujari  A V R Reddy
Institution:1. Analytical Chemistry Division, Bhabha Atomic Research Centre, Trombay, Mumbai, 400085, India
2. Radiochemistry Division, Bhabha Atomic Research Centre, Trombay, Mumbai, 400085, India
3. NCCCM, Bhabha Atomic Research Centre, Hyderabad, 500062, India
Abstract:Boron is an important element in nuclear technology. A comparative study was carried out for the determination of boron in borosilicate glass, boron carbide and graphite samples by wet-chemical and nuclear analytical methods. Wet chemical methods namely titrimetry, Inductively Coupled Plasma Mass Spectrometry and ICP Optical Emission Spectrometry and nuclear analytical methods namely Particle Induced Gamma-Ray Emission and Nuclear Reaction Analysis were used. Boron concentrations were in trace (mg kg?1) level in graphite and percentage level in borosilicate glass and boron carbide.
Keywords:
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