Synthesis and Hydrolysis of Hybridized Silicon Alkoxide: Si(OEt)x(OBut)4-x. Part II: Hydrolysis of the Si(OEt)x(OBut)4-x |
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| Authors: | Bing Cao Zuyi Zhang Congshan Zhu |
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| Affiliation: | (1) Shanghai Institute of Optics and Fine Mechanics, Academia Sinica, Shanghai, 201800, P.R.China, P.O. Box, 800-211 |
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| Abstract: | The hydrolyzation behavior of the Si(OEt)x(OBut)4-x synthesized in part I was investigated by gas chromatogram/mass spectrum (GC/MS) technique. In the Si(OEt)x(OBut)4-x, Si(OEt)(OBut)3 showed more rapid hydrolysis than Si(OEt)2(OBut)2, especially in the initial stages of the hydrolyzation. The dimer and trimer formations along with the sol-gel course were followed during the hydrolyzation process. |
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| Keywords: | hybridized silicon alkoxide gas chromatogram/mass spectrum hydrolysis |
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