Synthesis and Crystal Structure of a Depside Derivative 2-(2-Methoxy-2-oxoethyl)phenyl 2-(3,4-Dimethoxyphenyl)acetate |
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| Authors: | Peng-Cheng Lv Kai-Rui Wang Wen-Jun Mao Rui-Qin Fang Jin Chen Jing Xiong Hai-Liang Zhu |
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| Institution: | (1) Key Laboratory of Anhui Educational Department, Anhui University of Technology, 243002 Maanshan, People’s Republic of China;(2) State Key Laboratory of Pharmaceutical Biotechnology, Nanjing University, 210093 Nanjing, People’s Republic of China; |
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| Abstract: | Abstract A depside derivative, 2-(2-methoxy-2-oxoethyl)phenyl 2-(3,4-dimethoxyphenyl)acetate (3), was synthesized through a facile approach in high yields. Its structure was confirmed by 1H NMR, 13C NMR, ESI mass spectra, elemental analyses and X-ray single crystal diffraction study. Crystal structure analysis revealed
that compound 3 crystallized in the monoclinic, space group P21/c with the following unit cell parameters: a = 10.173(2) Å, b = 10.459(2) Å, c = 16.516(3) Å, α = 90°, β = 102.30(3)°, γ = 90°, V = 1717.0(6) Å3, Z = 4. |
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