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Synthesis of 2-substituted 3,4-bis(diethoxyphosphorylmethyl)furans |
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| Authors: | Pevzner L. M. |
| Affiliation: | 1.St. Petersburg State Technological Institute (Technical University), Moskovskii pr. 26, St. Petersburg, 190031, Russia ; |
| Abstract: | Bromination of ethyl 4-(diethoxyphosphorylmethyl)-5-methylfuran-2-carboxylate and 4-(diethoxyphosphorylmethyl)-5-methylfuran-2-carbonitrile with N-bromosuccinimide followed by phosphorylation via the Arbuzov reaction have yielded the corresponding 2-substituted 4,5-bis(diethoxyphosphorylmethyl)furans. Synthesis and transformations of bisphosphorylated 2-furoic acid and its derivatives are described. |
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