Characterization and Comparative Studies on Conventional and Microwave Synthesis of Some Disulfides |
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| Authors: | Nalan Turkoz Karakullukcu Hasan Yakan Seyhan Ozturk Halil Kutuk |
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| Affiliation: | Chemistry Department, Faculty of Arts and Sciences , Ondokuz Mayis University , Atakum , Samsun , Turkey |
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| Abstract: | Abstract Some disulfide derivatives have been prepared by microwave assisted synthesis methodology from thiophthalimides(sulfenimides) and thiols in a modified microwave oven under reflux at 600 Watt in ethanol. Elucidation of the structures of the synthesized compounds has been performed by IR, 1H NMR, and 13C NMR spectroscopic methods. [Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements for the following free supplemental files: Additional figures] |
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| Keywords: | Disulfides cysteine 2-mercaptobenzimidazole 2-mercaptonicotinic acid microwave heating |
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