Characterization and Comparative Studies on Conventional and Microwave Synthesis of Some Disulfides |
| |
| Authors: | Nalan Turkoz Karakullukcu Hasan Yakan Seyhan Ozturk Halil Kutuk |
| |
| Institution: | Chemistry Department, Faculty of Arts and Sciences , Ondokuz Mayis University , Atakum , Samsun , Turkey |
| |
| Abstract: | Abstract Some disulfide derivatives have been prepared by microwave assisted synthesis methodology from thiophthalimides(sulfenimides) and thiols in a modified microwave oven under reflux at 600 Watt in ethanol. Elucidation of the structures of the synthesized compounds has been performed by IR, 1H NMR, and 13C NMR spectroscopic methods. Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements for the following free supplemental files: Additional figures] |
| |
| Keywords: | Disulfides cysteine 2-mercaptobenzimidazole 2-mercaptonicotinic acid microwave heating |
|
|
