Optically Active Phenyl-t-Butylphosphinothioic Acid as a Useful CSA for the Enantiomeric Excess Determination of Alcohols,Aminoalcohols and Related Compounds |
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| Authors: | Jan Omelańczuk |
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| Affiliation: | Centre of Molecular and Macromolecular Studies, Polish Academy of Sciences , 90-363 Lód?, Sienkiewicza, 112, POLAND |
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| Abstract: | Abstract There are rather few methods for determination of the enantiomeric excess of chiral alcohols, amines, thiols and related compounds.1 All these methods consist in the formation of. diastereomeric derivatives of the samples investigated with various chiral derivatizing agents (the CBA method) followed by the quantitative determination of their diastereomer composition using NMR or other techniques. |
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