Synthesis and Study of Spatial Structure 3,7-Bis(Dimethylamino)-5,10-Dihydrodibenzo-[b,e]- Phosphorines by NMR |
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| Authors: | V V Negrebetskii I N Pervukhina B I Stepanov |
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| Institution: | 1. All-Union Scientific Research Institute of Plant Protecting Chemicals , Ugreshskaya 33, Moscow , 109088 , USSR;2. Moscow D.I. Mendeleyev Institute of Chemical Technology , Miusskaya 9, Moscow , 125820 , USSR |
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| Abstract: | Abstract The phosphorines (VIII-XI) were obtained in the reaction 3,3-bis(dimethylamino)triphenylphosphine (I) and bis(3-dimethylaminophenyl) pentafluorophenylphosphorine (II) with benzaldehyde (III) and its 4-methoxy (IV), 4-dimethylamino (V), 2-fluro (VI), pentafluoro (VII) derivatives according to the scheme (1). |
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