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Characterization of tungsten tips for STM by SEM/AES/XPS
Authors:W Lisowski  A H J van den Berg  G A M Kip and L J Hanekamp
Institution:(1) Faculty of Applied Physics, University of Twente, P. O. Box 217, NL-7500 AE Enschede, The Netherlands;(2) Centre of Material Research, University of Twente, P. O. Box 217, NL-7500 AE Enschede, The Netherlands;(3) Present address: Institute of Physical Chemistry, Polish Academy of Sciences, ul. Kasprzaka 44/52, PL-01-224 Warszawa, Poland
Abstract:Summary For the first time, both X-ray Photoelectron Spectroscopy (XPS) and Auger Electron Spectroscopy (AES) techniques were applied in analysis of surface contamination of electrochemically etched Scanning Tunneling Microscope (STM) tungsten tips. Carbon monoxide, graphite, tungsten carbide and tungsten oxide were found as main surface contaminations of STM tungsten tips. The thickness of tungsten oxide layers was estimated to be about 1–3 nm. Quantitative analysis of surface and bulk concentration of carbon, oxygen and tungsten has been performed.
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