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Low temperature solventless synthesis and characterization of Ni and Fe magnetic nanoparticles
Authors:Liis Seinberg  Shinpei Yamamoto  Ruwan Gallage  Masahiko Tsujimoto  Yoji Kobayashi  Seiji Isoda  Mikio Takano  Hiroshi Kageyama
Affiliation:Department of Energy and Hydrocarbon Chemistry, Graduate School of Engineering, Kyoto University, Nishikyo-ku, Kyoto, 615-8510, Japan.
Abstract:We have successfully implemented a facile, one-pot solventless synthesis procedure starting from acetylacetonate salts and CaH(2) to obtain carbon-coated ferromagnetic metallic Ni and Fe nanoparticles at low temperature. The use of CaH(2) as a reductant drastically reduces reaction temperature down to 140 °C.
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