| 气相色谱法测定羟乙基乙二胺中的乙二胺含量 |
| |
| 引用本文： | 段钢,孙伏恩. 气相色谱法测定羟乙基乙二胺中的乙二胺含量[J]. 分析测试技术与仪器, 2009, 15(4): 238-240 |
| |
| 作者姓名： | 段钢 孙伏恩 |
| |
| 作者单位： | 广州天赐高新材料股份有限公司,广东,广州,510760 |
| |
| 摘 要： | 采用毛细管气相色谱内标法测定羟乙基乙二胺中的乙二胺含量．结果表明。乙二胺在0．12．0ms／mL范围内的线性关系良好（r=0．9997），检出限为0．02m/mL，方法的精密度RSD为1．7％（n=6），加标回收率在95％～101％．
|
| 关 键 词： | 羟乙基乙二胺 乙二胺 气相色谱法 内标法 |
| 收稿时间： | 2009-08-13 |
| 修稿时间： | 2009-09-24 |
Determination of Ethylenediamine in 2-(2-Aminoethylamino) Ethanol by Gas Chromatography |
| |
| DUAN Gang and SUN Fu-en. Determination of Ethylenediamine in 2-(2-Aminoethylamino) Ethanol by Gas Chromatography[J]. Analysis and Testing Technology and Instruments, 2009, 15(4): 238-240 |
| |
| Authors: | DUAN Gang and SUN Fu-en |
| |
| Affiliation: | DUAN Gang,SUN Fu-en(Guangzhou Tinci High-Tech Materials Co,Guangzhou 510760,China) |
| |
| Abstract: | Ethylenediamine in 2-(2-Aminoethylamino) ethanol was determined by capillary gas chromatography with internal standard method.The results showed that calibration curves presented good linear relationship in the range of 0.1~2.0 mg/mL with a correlation coefficient of 0.9997.The detection limit of the method was 0.02 mg/mL.The relative standard deviation(RSD)of the method was 1.7%(n=6).The recovery achieved 95%~101%. |
| |
| Keywords: | 2-(2-Aminoethylamino) ethanol ethylenediamine gas chromatography internal standard |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《分析测试技术与仪器》浏览原始摘要信息 |
|
点击此处可从《分析测试技术与仪器》下载全文 |
