| 金属有机化合物中过渡金属的原子吸收分光光度法测定 |
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| 引用本文： | 蔡起秀,朱善山,薛长发. 金属有机化合物中过渡金属的原子吸收分光光度法测定[J]. 有机化学, 1982, 0(4) |
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| 作者姓名： | 蔡起秀 朱善山 薛长发 |
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| 作者单位： | 中国科学院上海有机化学研究所，876所，中国科学院上海有机化学研究所 |
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| 摘 要： | 本文报导应用火焰原子吸收分光光度法对金属有机化合物中过渡金属铜、镍、钴、铁、钼及铬的定量测定。我们将金属有机化合物溶解在适当的有机溶剂或水中,不必分离基体,即可用标准加入法直接进行测定。操作简单,速度快,相对误差<0.4％。
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| 关 键 词： | 原子吸收分光光度法 元素分析 过渡元素 有机金属化合物 |
Determination of Transition Metals in Organometailic Compounds by Atomic Absorption Spectrophotometry |
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| Cai Qixiu,Zhu Shanshan,Xue Changfa. Determination of Transition Metals in Organometailic Compounds by Atomic Absorption Spectrophotometry[J]. Chinese Journal of Organic Chemistry, 1982, 0(4) |
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| Authors: | Cai Qixiu Zhu Shanshan Xue Changfa |
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| Affiliation: | Cai Qixiu,Zhu Shanshan,Xue Changfa Shanghai Institute of Organic Chemistry,Academia Sinica |
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| Abstract: | The determination of transition metals in a variety of organometalliccompounds by atomic absorption spectrophotometry has been investigated.Thismethod involves direct estimation of metals in solution,prepared by dissolving thesample either in suitable organic solvent or in deionized water.Addition of stan-dard was used in the analysis.It is simple,rapid,and gives a good result with rela-tive error <0.4%. |
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| Keywords: | atomic absorption spectrophotometry elemental analysis transition element organometallic compound. |
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