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Temperature program optimization by computer simulation for the capillary GC analysis of fatty acid methyl esters on biscyanopropyl siloxane phases
Authors:Erkki Sippola  Frank David  Pat Sandra
Abstract:The selectivity of capillary columns coated with biscyanopropyl siloxane stationary phases for the separation of fatty acid methyl esters has been optimized by means of computer-assisted column temperature optimization software. Temperature programming rates yielding the highest resolution in the shortest analysis time were selected for split, splitless, and on-column injection operated in the constant pressure and pressure programmed modes.
Keywords:Capillary GC  Biscyanopropyl siloxane phases  Temperature program optimization  Computer simulation (Drylab GC)  Fatty acid methyl esters  Electronic pressure control
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