1,4-Cyclohexadiene with Pd/C as a rapid, safe transfer hydrogenation system with microwave heating |
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| Authors: | John F Quinn Dana A Razzano Kathryn C Golden Brian T Gregg |
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| Institution: | AMRI, Medicinal Chemistry Department, 26 Corporate Circle, PO Box 15098, Albany, NY 12212-5098, USA |
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| Abstract: | A method for the rapid, safe hydrogenation of alkenes and deprotection of benzyl ethers and carboxybenzyl amides is described using catalytic transfer hydrogenation under microwave heating conditions. Commonly available Pd/C catalyst is extremely effective with 1,4-cyclohexadiene as the hydrogen transfer source. In general, the reactions are complete within five minutes at 100 °C. |
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| Keywords: | Transfer hydrogenation Palladium on carbon 1 4-Cyclohexadiene Microwave |
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