Vibrational study of tin-containing siloxane ring compounds |
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| Authors: | Amal Haoudi-Mazzah Ahmed Mazzah Paul Dhamelincourt |
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| Institution: | Laboratoire de Spectrochimie Infrarouge et Raman, CNRS UP 2631L, Université des Sciences et Technologie de Lille, 59655 Villeneuve d’Ascq cedex, France |
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| Abstract: | By a condensation reaction of (t-Bu)2Si(OH)2 (L) with tin tetrachloride (SnCl4), two different compounds were obtained: a condensation product between two molecules of L and a tin-containing siloxane bicycloheptane ring compound formed by a subsequent reaction between partially hydrolysed SnCl4 and L. The latter was identified by x-ray diffraction. The Raman spectra of both isolated compounds were recorded and confirmed the structure obtained for the ring compound. © 1997 John Wiley & Sons, Ltd. |
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